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Hope
College Department of Physics and Engineering Research Experiences for Undergraduates Summer 2006 Project Summary |
| Project Title: | Trace Elemental Analysis Of Glass Via PIXE |
| Student Name: | Chris Hall (with Derek Padilla) |
| Student's Home Institution: | Hope College |
| Research Advisor: | Dr. Paul DeYoung and Dr. Graham Peaslee |
| Source of Support: | National Science Foundation under Grant Numbers 0354920 and 0319523. |
Using the Hope College Ion Beam Analysis Laboratory (HIBAL), protons with an energy of 2.3 MeV are accelerated towards the prepared samples in an evacuated target chamber. Resultant x-rays are detected at 45º with a Si(Li) detector. The x-ray spectra are analyzed with the GUPIXWIN peak-fitting software which outputs relative concentrations of trace elements. With these relative concentrations, ratios between trace elements are used for the comparative aspect of the statistics. This use of ratios eliminates much systematic error that arises when trying to acquire absolute concentrations. Specific ratios between samples are compared using Z-score testing which gives a scale of the difference between the two samples for that particular elemental ratio. When comparing two hits on the same sample, there still remains a difference in the trace elemental concentrations of that same sample due to statistical errors. This difference is used as a control in our evaluations of unknown sample concentrations. To obtain reliable statistics, multiple spectra are always obtained on each sample.
*This material is based upon work supported by the National
Science Foundation under NSF-REU Grant No. 0452206
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Publications and Presentations:
"
Comparison
of Glass Fragments Using Particle Induced X-Ray Emission (PIXE) Spectrometry."
P.A. DeYoung, P.J. Mears*, C.C. Hall*, D.J. Padilla*, R.A. Sampson*, and G.F.
Peaslee.
Scheduled for publication in the Journal of
Forensic Sciences, (2011).
“Forensic Analysis of Tempered Sheet Glass by Particle Induced X Ray
Emission (PIXE)” L. J. Jisonna, P. A. DeYoung, J. Ferens*, C. Hall*,
J. M. Lunderberg*, P. Mears*, D. Padilla*, G. F. Peaslee, and R. Sampson*.
Nucl. Instr. And Meth. B, Nucl. Instr. And Meth. B (2011).
“Spectroscopy of 13Li”, E.M. Lunderberg*, C.C. Hall*, P.A. DeYoung, M. Thoennessen, J. Snyder, and Mona Collaboration. Division of Nuclear Physics of the APS meeting, East Lansing MI, October 2011.
"First observation of excited states in 12Li" C.C. Hall*,
E.M. Lunderberg*, P.A. DeYoung, T. Baumann, D. Bazin, G. Blanchon, A. Bonaccorso,
B.A. Brown, J. Brown, G. Christian, D.H. Denby*, J. Finck, N. Frank, A. Gade,
J. Hinnefeld, C.R. Hoffman, B. Luther, S. Mosby, W.A. Peters, A. Spyrou, and
M. Thoennessen. Phys. Rev. C 81, 021301(R) (2010).
"Efficiency of the Modular Neutron Array (MoNA)." W.A.
Peters, T. Baumann, G.A. Christian, D.Denby*, P.A. DeYoung, J.E. Finck, C.C.
Hall*,
J. Hinnefeld, A. Schiller, M.J. Strongman, and M. Thoennessen. Proceedings
of the 20th International Conference of the Application of Accelerators in
Research and Industry CAARI 2008, AIP Conference Proceedings 1099,
807 (2009).
"Spectroscopy of 12Li." E. Lunderberg*,
C. Hall*, P. DeYoung, A. Spyrou, M. Thoennessen, MoNA Collaboration. CEU Poster
GB0.00070. Bull.
Am. Phys. Soc. 54,
(2009). Division of Nuclear Physics Fall Meeting. Waikoloa, Hawaii (2009).
"Production
of Nuclei in Neutron Unbound States via Primary Fragmentation of 48Ca",
G. Christian, W.A. Peters, D. Absalon*, D. Albertson*, T. Baumann, D. Bazin,
E. BreitbachI, J. Brown, P.L. Cole*, D.
Denby*, P.A. DeYoung, J.E. Finck, H. Frank, A. Fritsch*, C. Hall*, A.M. Hayes,
J. Hinnefeld, C.R. Hoffman, R. Howes, B. Luther, E. Mosby*, S. Mosby*, D. Padilla*,
P.V. Pancella, G. Peaslee, W.F. Rogers, A. Schiller, M.J. Strongman, M. Thoennessen,
and L.O. Wagner*. Nucl. Phys. A801, 101, (2008).
"Ground Stake Energy and Width of
the 7He from 8Li
Proton Knockout." D.L. Denby*, P.A. DeYoung, T. Baumann, D. Bazin,
E. Breitback*, J. Brown, N. Frank, A. Gade, C.C. Hall*, J. Hinnefeld, C.R.
Hoffman, R. Howes, R.A. Jenson*, B. Luther, S.M. Mosby, C.W. Olson*, W.A.
Peters, A. Schiller, A. Spyrou, and M. Thoennessen. Phys. Rev. C 78,
044303 (2008).
"Development of an Ion Beam Analysis Method for Forensic
Analysis of Glass", Richard Sampson*, Graham F. Peaslee, Paul A. DeYoung,
Christopher Hall*, Derek Padilla*, and Patrick Mears*. American Academy of
Forensic Sciences 2008 Annual Meeting, Denver, Colorado, (2008).
"Studying the structure of the neutron-unbound 12Li." A.
Spyrou, M. Thoennessen, P.A. DeYoung, C.C. Hall*, and the MoNA Collaboration.
Paper ED.00006. Bull. Am. Phys. Soc. 53, 65 (2008). Division
of Nuclear Physics Fall Meeting. Oakland, CA, October 2008. "Experimental Observation
of Decay Energy of 12,13Li." C. Hall*, P.A. DeYoung, S. Mosby,
A. Spyrou, and M. Thoennessen. CEU Poster DA.00037.
Bull. Am. Phys. Soc. 53, 46 (2008). Division of nuclear Physics
Fall Meeting. Oakland, CA, October 2008. "Development
of an Ion Beam Analysis Method for Forensic Analysis of Glass."Richard
Sampson*, Graham F. Peaslee, Paul A. DeYoung, Christopher
Hall*, Derek Padilla*, and Patrick Mears*. American Academy of Forensic Sciences
2008 Annual Meeting, Washington D.C. 2008.
"Breakup of 6He Incident on 209Bi
Near the Coulomb Barrier", J.J. Kolate, H. Amro, F.D. Becchetti, J.A.
Brown, P.A. DeYoung, M. Hencheck, J.D. Hinnefeld, G.F. Peaslee, A.L. Fritsch,
C. Hall*, U. Khadka*, Patrick J. Mears*, P. O'Rourke, D. Padilla*, J. Reith*,
Tabatha Spencer, and T. Williams. Phys Rev. C 75, 031302 (2007).