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Hope
College Physics Department Research Experiences for Undergraduates Summer 2011 Project Summary |
| Project Title: | Comparative Analysis of Forensic Glass |
| Student Name: | Curtis Johnson |
| Student's Home Institution: | University of Wisconsin Eau Claire |
| Research Advisor: | Dr. Paul DeYoung and Dr. Graham Peaslee |
| Source of Support: | This work is supported by the National Science Foundation under NSF-REU Grant No. PHY/DMR-1004811. |
The current process for elemental analysis of glass, laser ablation ICP, is
destructive and time consuming. Part of the sample must be ablated, destroying
the piece of glass; this can be a hindrance when working with limited glass
from a crime scene. Alternatively, Particle Induced X-ray Emission (PIXE) is
an ion beam analysis technique that uses a particle accelerator to analyze
the chemical composition of a sample from emitted X-rays. PIXE is a completely
non-destructive method, which is less time consuming than ICP. This makes PIXE
a viable option to presort glass obtained at a crime scene. Concentrations
of six elements (Ca, Ti, Mn, Fe, Sr, and Zr) were investigated. Extreme care
was taken to eliminate systematic error present in the experiment. Variation
in both absolute and calcium normalized levels of these elements were compared
demonstrating that PIXE can be used on its own to identify the possibility
that two samples have come from the different provenance.
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